By Magrone P., Servadei R.
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Extra info for A stability result for mountain pass type solutions of semilinear elliptic variational inequalities
When the unit has reached room temperature, disconnect the cooling hoses, backflush the column with water then remove the top end from the boiler for cleaning. Now that we know how to run the still, it might be a good idea to give some more thought of how to optimize the distillation. 28 B U I L D I N G A H O M E Column Tuning D I S T I L L A T I O N A P P A R A T U S Whenever you try to maximize the purity of the distillate in the least amount of time, you have to deal with the amount of refluxing needed.
It’s also important to recognize that no matter how many reflux cycles are applied to the process, you will never be able to get a completely pure distillate. Under the circumstances then, your goal in operating the still should be to produce a purer product than what you can buy commercially, and at the same time produce the product at the least cost. ”. The system we are building controls the reflux ratio by regulating the cooling flow inside the column. We calculate the reflux ratio by measuring the maximum distillation rate at a given heat level without cooling, and then regulate the cooling to provide an appropriate fraction of that rate.
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A stability result for mountain pass type solutions of semilinear elliptic variational inequalities by Magrone P., Servadei R.